Synthesis, characterization, FTIR and UV-Vis of a novel
(E)-3-(5-bromo-3-fluoro-2-hydroxybenzilide amino)benzaldehyde
- Received: July, 28, 2024
- Revised: October, 14, 2024
- Accepted for publication: October, 14, 2024
- DOI 10.26902/JSC_id139026
- EDN: REGOYW
- Views: 150
1 Department of Physics, Faculty of Science, Atatürk University, Erzurum, Turkey
2 Department of Physics, Faculty of Sciences, Ondokuz Mayıs University, Atakum, Samsun, Turkey
3 Department of Chemistry, Faculty of Science, Gebze Technical University, Gebze, Turkey
4 Department of Chemistry, Faculty of Sciences, Ondokuz Mayıs University, Atakum, Samsun, Turkey
One of the most studied compound families in the field of crystallography is the Schiff-based compounds. The basis of this research article is a newly synthesized Schiff-base compound. This research aims to investigate the synthesized (E)-3-(5-bromo-3-fluoro-2-hydroxybenzilide amino)benzaldehyde phenol compound using experimental methods. FTIR, UV-Vis and X-ray diffraction methods were used to elucidate the structural properties of the compound synthesized at the end of chemical processes. The structure solution was carried out from the data obtained as a result of X-ray analysis. According to these results, a molecule was formed in the asymmetric cell. The resulting structure has shaped in enol-imine form. The number of molecules in the unit cell was also determined as 4 (Z = 4). According to
the results obtained as a result of UV-Vis spectroscopy, the structure revealed
that the enol-imine form was dominant. The reasons for this situation were
explained.
Keywords: X-ray diffraction, UV-Vis and Schiff base
|
Импакт-фактор 2025 1.5 |
||||
|
Срок опубликования 4 мес |
||||
|
100-лет со дня рождения
Электронный спецвыпуск, |
Уважаемые авторы и подписчики “Журнала структурной химии”,
в свободном доступе
архив ЖСХ до 2022 года ("Номера").
Спецвыпуски
Самое интересное
Статьи, к которым чаще всего обращаются посетители
Рубрики